Ausstattung und Methoden
Large Scale facilities:
XPS and ToF-SIMS Technology cluster at KNMF
Synchrotron Powder diffraction at Petra III, beamline P02.1 (cooperation)
Neutron powder diffraction at FRM II, beamline SPODI (cooperation)
Laboratories an Equipment:
Lab-infrastructure
- Chemistry lab space with 9 fume hoods
- 7 Ar-gloveboxes
- Several tube, muffle, induction and arc-melting furnaces and hydrothermal synthesis chambers
- Ball mills , centrifuges
- 1000 tons multianvil press for high pressure/high temperature syntheses 18 GPa, 2800 K (Voggenreiter)
- Electrospinner EC-CLI (IME Technologies)
Bulk Characterization
- X-ray powder diffraction with Mo, Cu and Co wavelength with different geometries and sample environment
- Simultaneous Thermal Analysis (TG-DTA/DSC) with combined FT-IR gas analysis operated under Ar-atmosphere (Netzsch Jupiter 449 C)
- PPMS
Spectroscopy
- Raman microscope type HORIBA LabRam Evolution HR (Laser wavelengths: HeNe-Laser (633 nm, 17 mW), Nd:YAG solid state (523 nm, 100 mW), diode laser (473 nm, 25 mW)
- Bruker Tensor 27 FT-IR spectrometer attached to STA and operated under Ar-atmosphere
Electrochemical Characterization
- Several Potentiostats with 192 channels
- Climate chambers
- 5 Redox flow battery test stations (Fuelcon, Greenlight Innovations, Scribner)
Microscopy
- Optical microscope Leica M205
- FE-SEM MERLIN microscope (Zeiss GmbH)
- EM ACE 600 coater (Leica)
Surface Characterization
- K-Alpha XPS instrument with integrated glove-box for atmosphere contact free sample handling (Thermo Fisher Scientific)
- VG ESCA5 XPS Spectrometer equipped with Alpha 110 electron energy analyzer (Thermo Fisher Scientific)
- ToF.SIMS 5 spectrometer (ION-TOF GmbH)
- DektakXT Stylus Profilometer (Bruker AXS)
- Z400 3-magnetron (PK75) sputtering system for multi-layer deposition (Leybold)
- 3 UHV-sputter setups equipped with 3” planar magnetrons
Equipment and Methods
Large Scale facilities:
XPS and ToF-SIMS Technology cluster at KNMF 
Synchrotron Powder diffraction at Petra III, beamline P02.1 (cooperation)
Neutron powder diffraction at FRM II, beamline SPODI (cooperation)
Laboratories an Equipment:
Lab-infrastructure
- Chemistry lab space with 9 fume hoods
- 7 Ar-gloveboxes
- Several tube, muffle, induction and arc-melting furnaces and hydrothermal synthesis chambers
- Ball mills , centrifuges
- 1000 tons multianvil press for high pressure/high temperature syntheses 18 GPa, 2800 K (Voggenreiter)
- Electrospinner EC-CLI (IME Technologies)
Bulk Characterization
- X-ray powder diffraction with Mo, Cu and Co wavelength with different geometries and sample environment
- Simultaneous Thermal Analysis (TG-DTA/DSC) with combined FT-IR gas analysis operated under Ar-atmosphere (Netzsch Jupiter 449 C)
Spectroscopy
- Raman microscope type HORIBA LabRam Evolution HR (Laser wavelengths: HeNe-Laser (633 nm, 17 mW), Nd:YAG solid state (523 nm, 100 mW), diode laser (473 nm, 25 mW)
- Bruker Tensor 27 FT-IR spectrometer attached to STA and operated under Ar-atmosphere
Electrochemical Characterization
- Several Potentiostats with 192 channels
- Climate chambers
- 5 Redox flow battery test stations (Fuelcon, Greenlight Innovations, Scribner)
Microscopy
- Optical microscope Leica M205
- FE-SEM MERLIN microscope (Zeiss GmbH)
- EM ACE 600 coater (Leica)
Surface Characterization
- K-Alpha XPS instrument with integrated glove-box for atmosphere contact free sample handling (Thermo Fisher Scientific)
- VG ESCA5 XPS Spectrometer equipped with Alpha 110 electron energy analyzer (Thermo Fisher Scientific)
- ToF.SIMS 5 spectrometer (ION-TOF GmbH)
- DektakXT Stylus Profilometer (Bruker AXS)
- Z400 3-magnetron (PK75) sputtering system for multi-layer deposition (Leybold)
- 3 UHV-sputter setups equipped with 3” planar magnetrons